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Characterization of triglycerides isolated from jojoba oil
Authors:M Van Boven  R A Holser  M Cokelaere  E Decuypere  C Govaerts  J Lemey
Affiliation:(1) Laboratory of Toxicology and Food Chemistry, Katholieke Universiteit Leuven, B-3000 Leuven, Belgium;(2) New Crops Research, USDA, ARS, NCAUR, 61604 Peoria, Illinois;(3) Interdisciplinary Research Center, Katholieke Universiteit Leuven, Campus Kortrijk, B-8500 Kortrijk, Belgium;(4) Laboratory of Physiology and Immunology of Domestic Animals, Katholieke Universiteit Leuven, B-3000 Leuven, Belgium;(5) Laboratory of Pharmaceutical Chemistry, Katholieke Universiteit Leuven, B-3000 Leuven, Belgium
Abstract:Triglyceride compounds isolated from jojoba seed oil by column chromatography were composed predominantly of C18′ C20′ C22′ and C24 n−9 fatty acids with minor amounts of saturated C16. Chain length and double-bond positions were determined by gas-liquid chromatography and gas-liquid chromatography-mass spectrometry of the corresponding methyl ester and picolinyl ester derivatives. Triglyceride structures were analyzed directly by ion trap mass spectrometry. The analysis of minor compounds, can provide highly specific information about the identity of an oil.
Keywords:GC-MS  ion trap MS  jojoba  triglycerides  wax ester
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