| 氟虫腈高效液相色谱分析方法的研究 |
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| 引用本文： | 武中平,高巍,颜春荣,张晓强. 氟虫腈高效液相色谱分析方法的研究[J]. 现代农药, 2006, 5(2): 21-23 |
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| 作者姓名： | 武中平 高巍 颜春荣 张晓强 |
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| 作者单位： | 国家农药产品质量监督检验中心(南京),南京,210029 |
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| 基金项目： | 江苏省技术监督局课题(NO:KJ031610) |
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| 摘 要： | 对氟虫腈高效液相色谱分析方法进行了研究。用紫外检测器、C18柱,以乙腈+甲醇+水为流动相(体积比为40:38:22),对氟虫腈的分析可取得满意的效果。该方法的相对标准偏差为0.42%,添加平均回收率为100.5%～104.3%。
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| 关 键 词： | 氟虫腈 C18 紫外检测器 |
| 文章编号： | 1671-5284（2006）02-0021-03 |
| 收稿时间： | 2006-01-06 |
| 修稿时间： | 2006-01-06 |
Study on the Method of HPLC for Fipronil |
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| WU Zhong-ping,GAO Wei,YAN Chun-rong,ZHANG Xiao-qiang. Study on the Method of HPLC for Fipronil[J]. Modern Agrochemicals, 2006, 5(2): 21-23 |
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| Authors: | WU Zhong-ping GAO Wei YAN Chun-rong ZHANG Xiao-qiang |
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| Affiliation: | The National Quality Supervision and Inspection Center for Pesticide, Nanjing 210002, China |
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| Abstract: | Method of HPLC for fipronil was studied in this article. Fipronil was determined by HPLC with UV detector, ODS column and acetonitrile+methanol+water as mobile phase, the results was satisfactory. The determination results of HPLC showed that the relative standard deviations was 0.42% and average spiked recoveries of fipronil were within 100.5%–104.3%. |
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| Keywords: | fiprosil C18 UV detector |
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