| 工业反应过程的开发方法Ⅺ．炔醛法合成丁二醇反应过程的开发 |
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| 引用本文： | 毛之侯,张濂,顾其威.工业反应过程的开发方法Ⅺ．炔醛法合成丁二醇反应过程的开发[J].石油化工,1994(5). |
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| 作者姓名： | 毛之侯 张濂 顾其威 |
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| 作者单位： | 华东理工大学联合化学反应工程研究所 |
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| 摘 要： | 以炔醛法合成１，４一丁二醇反应的炔化反应过程和加氢反应过程为研究对象，应用工业反应过程开发方法的基本原则，进行炔化反应和加氢反应开发方法的论述，包括确定优选工艺条件、反应器型大的选择和反应器的主要工程问题。从小试、中试、冷漠试验到工业规模试验，为大型装置设计提供依据。
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| 关 键 词： | 1，4－丁炔二醇，1，4－丁醇，淤浆床，工艺开发，工艺放大 |
Methodology for the Development of Indnstrial Reaction Processes Ⅺ. The Process Development of 1,4-Butanediol Synthesis by Acetylene-formaldehyde Method |
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| Mao Zhihou,Zhang Lian and Cu Qiwei.Methodology for the Development of Indnstrial Reaction Processes Ⅺ. The Process Development of 1,4-Butanediol Synthesis by Acetylene-formaldehyde Method[J].Petrochemical Technology,1994(5). |
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| Authors: | Mao Zhihou Zhang Lian and Cu Qiwei |
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| Abstract: | The syntheSis of 1,4-butanediol by acetylenation and hydrogenation is presented in thispaper.The basic principles used for the process development methods of these industrial reac-tions are discussed,including optimization of reaction condition,selection of reactor typeand also the main engineering problems of the reactor considered.The study was done withlaboratory bench-scale,pilot-scale and finally industrial scale reactor,and a complete setof design information for large scale equipment was established. |
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| Keywords: | butyne-1 4-dio1 1 4-butanediol trickle-bed slurry-bed process development and scale-up |
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