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Effect of Thermal Treatment and Acid Leaching Process on Pore Characteristics of Nanometer Porous Glass
作者姓名:韩建军
作者单位:Key Laboratory
摘    要:Porous glass was prepared by thermally treating sodium borosilicate glass for different time, the effect of thermal treatment on pore size distribution was discussed and the pore size of the prepared porous glass was measured by scanning electron microscopy (SEM) and differential thermal analysis (DTA). The results show that the optimum porous glass with an average diameter of 80 nm can be prepared by thermal treatment at 600℃ for 12 h and then acid treatment for 12 h in 2 mol·L^-1 hydrochloric acid solution.

关 键 词:纳米级多孔玻璃  热处理  酸蚀刻过程  孔隙特性  相位分离  硼硅酸钠玻璃
收稿时间:2004-11-10
修稿时间:2006-05-28

Effect of thermal treatment and acid leaching process on pore characteristics of nanometer porous glass
Han?Jianjun,Xu?Feng,Liu?Jiandang,Zhao?Xiujian.Effect of Thermal Treatment and Acid Leaching Process on Pore Characteristics of Nanometer Porous Glass[J].Journal of Wuhan University of Technology. Materials Science Edition,2007,22(1):129-131.
Authors:Han Jianjun  Xu Feng  Liu Jiandang  Zhao Xiujian
Affiliation:(1) Key Laboratory of Silicate Materials Science and Engineering, Ministry of Education, Wuhan University of Technology, Wuhan, 430070, China
Abstract:Porous glass was prepared by thermally treating sodium borosilicate glass for different time, the effect of thermal treatment on pore size distribution was discussed and the pore size of the prepared porous glass was measured by scanning electron microscopy (SEM) and differential thermal analysis (DTA). The results show that the optimum porous glass with an average diameter of 80 nm can be prepared by thermal treatment at 600 °C for 12 h and then acid treatment for 12 h in 2 mol·L−1 hydrochloric acid solution. Funded by the National Natural Science Foundation of China (No.50302007), Chenguang Project of Wuhan(No.20055003059-7) and 2003 Opening Foundation of State Key Laboratory of Advanced Technology for Materials Synthesis and Processing.
Keywords:porous glass  thermal treatment  sodium borosilicate glass  phase-separate
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