| SnSb导电膜对钛基金属阳极涂层性能提高的深入研究 |
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| 引用本文： | 邹忠,李劼,张文根,丁凤其,肖劲,叶绍龙,周诗国,刘业翔. SnSb导电膜对钛基金属阳极涂层性能提高的深入研究[J]. 稀有金属, 2001, 25(3): 161-165 |
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| 作者姓名： | 邹忠 李劼 张文根 丁凤其 肖劲 叶绍龙 周诗国 刘业翔 |
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| 作者单位： | 中南大学冶金科学与工程系, |
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| 基金项目： | 国家自然科学基金资助项目(No.59804008) |
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| 摘 要： | 深入讨论了钛基金属阳极涂层制备中 ,在底层引入SnSb导电膜对其电催化性能提高的机理 ,并对影响电催化性能最重要的两个工艺参数 :温度和锑添加量进行了详细的研究。EDX面扫描结果表明 ,底层热分解成型的SbSn膜成分分布均匀 ,非常有利于DSA电催化性能的改善 ;X射线衍射结果证实了SnSb膜中主要以SnO2 和Sb2 O3相结构存在 ;对比实验得出了最佳工艺制备条件 :t=30 0℃ ,锑的添加量为 10 %。
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| 关 键 词： | SnSb导电膜 钛基金属阳极 电催化 |
| 文章编号： | 0258-7076(2001)03-0161-05 |
| 修稿时间： | 2000-04-25 |
Farther Research of Effectof Titanium-based Metal Anode Coating with SnSb Conducting Base Film |
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| ZOU Zhong,Li Jie,Zhang Wengeng,Ding Fengqi,Xiao Jing,Ye Shaolong,Zhou Shiguo,Liu Yexiang. Farther Research of Effectof Titanium-based Metal Anode Coating with SnSb Conducting Base Film[J]. Chinese Journal of Rare Metals, 2001, 25(3): 161-165 |
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| Authors: | ZOU Zhong Li Jie Zhang Wengeng Ding Fengqi Xiao Jing Ye Shaolong Zhou Shiguo Liu Yexiang |
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| Abstract: | The mechanism of improving electrocatalytic effect of titanium-based metal anode coating with SnSb conducting base film during the preparation was discussed. The most important preparing paramters,temperature and Sb additive were discussed in detail.The EDX results showed that the uniform distribution of coating constitute be benefit for the improvement of DSA electrocatalytic ability. The X ray results proved that the SnSb coating be mainly made up of SnO2 and Sb2O3 structure. The optimum preparing conditions, t=300℃ and 10% amount of Sb additives were acquired by the comparing experiments. |
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| Keywords: | SnSb conducting film Titanium based metal anode Electrocatalysis |
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