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钢中非金属夹杂物的三维定量表征
引用本文:严春莲,秦汉成,其其格,代锦,冯超,孟杨. 钢中非金属夹杂物的三维定量表征[J]. 金属热处理, 2023, 48(3): 280-286. DOI: 10.13251/j.issn.0254-6051.2023.03.047
作者姓名:严春莲  秦汉成  其其格  代锦  冯超  孟杨
作者单位:首钢集团有限公司技术研究院 检测中心, 北京 100043
摘    要:以超低碳钢、易切削钢、管线钢为研究对象,通过优化电解萃取法以及夹杂物自动分析技术,完成了钢中大尺寸氧化铝、大尺寸硫化锰、常规氧硫化物等典型夹杂物的三维形态表征及自动定量统计,并就滤膜干扰物、夹杂物分散状态、扫描电镜参数设置等影响夹杂物三维定量表征的因素进行了讨论。与二维分析相结合,夹杂物的三维形态表征及定量统计结果将提供最为全面、真实、准确的夹杂物信息。

关 键 词:夹杂物  三维表征  定量分析  
收稿时间:2022-10-27

Three-dimensional quantitative characterization of non-metallic inclusions in steels
Yan Chunlian,Qin Hancheng,Qi Qige,Dai Jin,Feng Chao,Meng Yang. Three-dimensional quantitative characterization of non-metallic inclusions in steels[J]. Heat Treatment of Metals, 2023, 48(3): 280-286. DOI: 10.13251/j.issn.0254-6051.2023.03.047
Authors:Yan Chunlian  Qin Hancheng  Qi Qige  Dai Jin  Feng Chao  Meng Yang
Affiliation:Testing & Analysis Center, Research Institute of Technology, Shougang Group Co., Ltd., Beijing 100043, China
Abstract:Three-dimensional morphological observation and statistical quantification of typical inclusions as large-size Al2O3, MnS and oxysulfides were conducted in the ultra-low carbon steel, the free cutting steel and the pipeline steel by using optimized electrolytic extraction and automated inclusion analysis technique. Some factors affecting the three-dimensional quantitative characterization of inclusions, such as the electrolytic interfering substance, the dispersion state of inclusions and the setting of SEM parameters were discussed about how to influence three-dimensional quantitative results. Combined with two-dimensional analysis, three-dimensional morphological observation and statistical quantification of the inclusions will provide more comprehensive, reliable and accurate information.
Keywords:inclusion  three-dimensional characterization  quantitative analysis  steel  
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