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水热热压法制备地质聚合物
引用本文:纪莹璐,宋慧平,程芳琴,张培华. 水热热压法制备地质聚合物[J]. 粉煤灰综合利用, 2014, 0(5): 22-25
作者姓名:纪莹璐  宋慧平  程芳琴  张培华
作者单位:1. 国家环境保护煤炭废弃物资源化高效利用技术重点实验室,山西大学资源与环境工程研究所,山西太原030006
2. 山西平朔煤矸石发电有限责任公司,山西平朔,036006
基金项目:山西省重大专项,国家科技支撑计划项目
摘    要:地质聚合物材料是一种新型的环保型无机复合材料,具有性能优越、价格低廉的特点.本研究采用水热热压技术,以粉煤灰、玻璃粉为主要原料,在200℃、8.5MPa的水热热压条件下制备粉煤灰基地聚合物材料.研究了不同碱激发剂的含量、浓度及玻璃粉添加量对材料抗压强度、收缩率的影响.结果表明,粉煤灰与玻璃粉的质量比为2∶1,添加25%的浓度为5 mol/L NaOH溶液时,固化体试样中有纤维状的地聚物生成,材料的抗压强度最高达到103.34MPa.

关 键 词:地质聚合物  粉煤灰  玻璃粉  水热热压技术

Preparation of Geopolymer Material by Hydrothermal Hot-pressing
Ji Yinglu,Song Huiping,Cheng Fangqin,Zhang Peihua. Preparation of Geopolymer Material by Hydrothermal Hot-pressing[J]. Fly Ash Comprehensive Utilization, 2014, 0(5): 22-25
Authors:Ji Yinglu  Song Huiping  Cheng Fangqin  Zhang Peihua
Affiliation:Ji Yinglu, Song Huiping, Cheng Fangqin, Zhang Peihua (1.Institute of Resources and Environment Engineering, State Environment Protection Key Laboratory of Efficient Utilization of Coal Waste Resources, Shanxi University, Taiyuan 030006, China; 2.Shanxi Pingshuo Gangue Power Generation Co., Ltd., Shuozhou 056800,China)
Abstract:The Geopolymer is a new type of environmentally friendly inorganic composite materials with the distinguishing features of superior performance and low price. Fly ash geopolymer material was prepared by hydrothermal hotK-pressing under standard conditions of 200℃ and 8.5 MPa. Experimental variables that affecting fly ash geopolymer's compressive strength, such as glass powder content, NaOH solution content,solution and concentration, were investigated. The optimum preparation conditions of geopolymer material were that the quality ratio of fly ash and glass powder is 2:1 and 25% NaOH solution (5 mol/L). Its compressive strength reached 103.34 MPa, which was the highest strength in this experiment range.
Keywords:Geopolymer  Fly ash  Glass powder  Hydrothermal hot-pressing technology
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