Changes in contributions of matrix and block boundary strengths to macroscopic hardness of high Cr ferritic steel during creep

The instrumented indentation test was applied to the interrupted creep specimens of turbine rotor steel (Fe-10Cr-1Mo-1W-VNbN) to investigate the changes in contributions of matrix and block boundary strengths to macroscopic hardness during creep. The indentation tests were performed under the loads of 1 and 10 mN to determine the matrix strength and the block boundary strength, respectively. The matrix strength of the grip portion decreased gradually with increasing life fraction and, for the gauge portion, the decrease was more pronounced, particularly, at the latter half of the life. On the other hand, the experimental results revealed that the block boundary strength decreased significantly at the early stage of the creep life, but this decrease was no longer pronounced when the creep life fraction exceeded 20%. Additionally, there was a good correlation between the block boundary strength and the width of block boundary carbide and the carbide coarsening was considered to be closely associated with the decrease in block boundary strength.