Synthesis of lanthanum zirconium oxide nanomaterials through composite-hydroxide-mediated approach |
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| Authors: | Hongyun Jin Dan Huang Qiang Gao Li Li Ning Wang Yongqian Wang Shuen Hou |
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| Affiliation: | 1. Faculty of Material Science and Chemistry Engineering, China University of Geosciences, Wuhan 430074, PR China;2. Engineering Research Center of Nano-Geomaterials of Ministry of Education, China University of Geosciences, Wuhan 430074, PR China;3. Qinghai Entry-Exit Inspection and Quarantine Bureau, PR China;1. Department of Chemistry, University of Pune, Ganeshkhind Road, Pune 411007, India;2. DST Unit on Nanoscience, Department of Physics, University of Pune, Ganeshkhind Road, Pune 411007, India;1. Radiochemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085, India;2. Fuel Chemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085, India |
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| Abstract: | A novel thermal barrier coating material, lanthanum zirconium oxide (La2Zr2O7) has been synthesized through the composite-hydroxide-mediated method at low temperature. The phase structures, morphology, thermal stability and thermal conductivity of the as-synthesized La2Zr2O7 were investigated systematically. The X-ray diffraction (XRD) patterns revealed a single phase with cubic pyrochlore structure for La2Zr2O7 after treated at 1300 °C for 100 h. The transmission electron microscope (TEM) and scanning electron microscope (SEM) analyses showed that the sample was made up of sphere-like nanoparticles with the size between 50 and 100 nm. Furthermore, the thermal analysis result demonstrated the La2Zr2O7 sample had high thermal stability even at 1300 °C. As the temperature increased to 1200 °C, the thermal conductivity value could be as low as 1.75 W m?1 K?1. Due to the high-temperature stability and lower thermal conductivity, the La2Zr2O7 material is expected to be a promising candidate for the use of thermal barrier coatings. |
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