| 苄达赖氨酸合成工艺的研究 |
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| 引用本文： | 朱忠华,刘玉华,徐新荣. 苄达赖氨酸合成工艺的研究[J]. 广东化工, 2012, 39(10): 17-18 |
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| 作者姓名： | 朱忠华 刘玉华 徐新荣 |
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| 作者单位： | 1. 武汉理工大学华夏学院,湖北武汉,430223
2. 湖北省医药学校,湖北武汉,430064 |
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| 摘 要： | 本篇文章对苄达酸与L-赖氨酸等摩尔反应制备苄达赖氨酸的工艺条件，用正交试验的方法，进行了优化，得出最佳反应温度及时间，产．品质量稳定；目标化合物的结构经核磁共振氢谱、碳谱、元素分析、红外光谱、质谱等确证：合成反应中使用的溶剂为乙醇，对环境小会产生污染，更适合工业化生产。
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| 关 键 词： | 苄达赖氨酸 合成 白内障 |
Study on Synthesis Process of Bendazac lysine |
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| Zhu Zhonghua,Liu Yuhua,Xu Xinrong. Study on Synthesis Process of Bendazac lysine[J]. Guangdong Chemical Industry, 2012, 39(10): 17-18 |
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| Authors: | Zhu Zhonghua Liu Yuhua Xu Xinrong |
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| Affiliation: | 1.Department of Pharmaceutical Engineering,Huaxia College,Wuhan University of Technology,Wuhan 430223;2.Hubei Pharmaceutical School,Wuhan 430064,China) |
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| Abstract: | The paper benzyl acid and L to reach-lysine,preparation of lysine benzyl Moore response technology conditions,Use orthogonal test method and optimized,The obtained optimum reaction temperature and time,stable and reliable product quality,The structures of the target molecules were confirmed by 1H NMR,13C NMR,elemental analysis,IR spectra and mass spectrum in our experiments,Use ethylalcohol for solvent in the reaction,it have not environmental pollution,it adapts industrialized production. |
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| Keywords: | bendazaclysine synthesis cataract |
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