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Improved additive manufacturing of silicon carbide parts via pressureless electric field-assisted sintering
Authors:Adam Bratten  Ruoyu Chen  Joshua Rittenhouse  Ming Leu  Haiming Wen
Affiliation:1. Department of Materials Science and Engineering, Missouri University of Science and Technology, Rolla, Missouri, USA;2. Department of Mechanical and Aerospace Engineering, Missouri University of Science and Technology, Rolla, Missouri, USA
Abstract:High solids loading silicon carbide (SiC)-based aqueous slurries containing only .5 wt. % organic additives were utilized to create specimens of various geometries via an extrusion-based additive manufacturing (AM) technique. Pressureless electric field-assisted sintering was performed to densify each specimen without deformation. The combination of these techniques produced parts with >98% relative density despite containing only 5 wt.% oxide sintering additives. After sintering, specimens contained only the α-SiC and yttrium aluminum perovskite phases. This suggests the evolution of a nonequilibrium yttrium aluminate phase, as well as transformation from β-SiC to α-SiC. The fabrication method presented in this work has advantages over other AM techniques commonly used with SiC, because it does not require significant organic additives nor additional postprocessing steps such as chemical vapor infiltration or polymer impregnation and pyrolysis.
Keywords:extrusion freeform fabrication  extrusion on demand  field-assisted sintering  silicon carbide
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