| 鱼油中多氯联苯的气相色谱-质谱(GC/MS)分析 |
| |
| 引用本文： | 许华,易荣,陈大舟,李蕾,方向. 鱼油中多氯联苯的气相色谱-质谱(GC/MS)分析[J]. 质谱学报, 2003, 24(1): 261-261 |
| |
| 作者姓名： | 许华 易荣 陈大舟 李蕾 方向 |
| |
| 作者单位： | 1. 北京化工大学,北京,100029
2. 国家标准物质研究中心,北京,100013 |
| |
| 摘 要： | 采用凝胶渗透色谱法 (GPC)和 Florisil土填充的 SPE小柱对鱼油样品进行净化处理 ,应用 GC/MS的分段选择性离子监测 (SIM)定性定量分析。结果表明 :SIM法可以定性分析鱼油实际样品中 3 1种多氯联苯 ,检测限为 1 0～ 1 0 0 fg,定量分析了其中的七种用来监测海洋受污染程度的多氯联苯
|
| 关 键 词： | 质谱学 多氯联苯分析 气相色谱-质谱(GC/MS) 鱼油 |
| 文章编号： | 1004-2997(2003)01-261-05 |
| 收稿时间： | 2002-10-22 |
| 修稿时间： | 2002-10-22 |
Determination of PCBs in Fish Oil by GC/MS |
| |
| XU Hua ,YI Rong ,CHEN Da-zhou ,LI Lei ,FANG Xiang. Determination of PCBs in Fish Oil by GC/MS[J]. Journal of Chinese Mass Spectrometry Society, 2003, 24(1): 261-261 |
| |
| Authors: | XU Hua YI Rong CHEN Da-zhou LI Lei FANG Xiang |
| |
| Affiliation: | XU Hua 1,YI Rong 2,CHEN Da-zhou 2,LI Lei 1,FANG Xiang 2 |
| |
| Abstract: | Fish oil sample is passed through GPC and SPE(Florisil)to be purified, and then determined by subsection SIM of GC/MS as quantitative analysis and qualitative analysis method. The results show that detection limit in the SIM mode is 10~100 fg. This method can determine 31 chromatogram peaks of PCBs qualitatively and 7 chromatogram peaks of PCBs quantitatively, which can be used to indicate how the marine has been contaminated. |
| |
| Keywords: | mass spectrometry analysis of PCBs GC/MS fish oil |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《质谱学报》浏览原始摘要信息 |
|
点击此处可从《质谱学报》下载全文 |
|
