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沉淀法制备ITO粉体及其性能研究
引用本文:谭翠,赵明勇,徐灿辉. 沉淀法制备ITO粉体及其性能研究[J]. 湖南有色金属, 2014, 30(6): 60-63
作者姓名:谭翠  赵明勇  徐灿辉
作者单位:柳州华锡铟锡材料有限公司,广西柳州,545006
摘    要:以InCl3、SnCl4、尿素和氨水为主要原料,采用化学共沉淀法制备出ITO粉体,探讨了沉淀剂种类和煅烧温度对ITO粉体性能的影响。结果表明:采用氨水可制备针状、粒度分布窄的纳米粉体,沉淀剂为尿素时则为块状、粒度分布较宽的微米粉体;随煅烧温度的提高,粉体的比表面积呈下降趋势,从700℃的28.65m2/g下降到900℃的12.23m2/g;氨水作沉淀剂且煅烧温度为700℃时可获得粒度均匀、分散性好、物相单一的纳米ITO粉。

关 键 词:共沉淀法  ITO粉体  微观形貌  粒径

Preparation and Properties of ITO Powder by Chemical Co-precipitation
TAN Cui,ZHAO Ming-yong,XU Can-hui. Preparation and Properties of ITO Powder by Chemical Co-precipitation[J]. Hunan Nonferrous Metals, 2014, 30(6): 60-63
Authors:TAN Cui  ZHAO Ming-yong  XU Can-hui
Affiliation:( LiuZhou China Tin Tin & Indium Material Co. ,Ltd,Liuzhou 545006, China)
Abstract:Using InC13 , SnC14, urea and ammonia as the main raw materials, ITO powders were prepared by chemical coprecipitation. The effect of precipitant and calcination temperature on the properties of ITO powder was investiga- ted. The results indicate that nanometer ITO powder with acicular morphology and a narrow size - distribution has been produced by ammonia, while ITO powder is block - shaped, reaching micrometer with a relatively wide size - distribution when urea was used. As calcination temperature increased from 700 ℃ to 900 ℃, surface area of the powder decreased from 28.65 m2/g to12.23 m2/g, showing a downward trend;nanometer ITO powder with uniform size, dispersion and sole phase could be made by ammonia under calcination temperature of 700 ℃.
Keywords:coprecipitation  ITO powder  microstructure  powder size
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