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MeV能量Si~+引起二次离子发射的研究
引用本文:祝兆文,郑涛,侯杰,聂锐,马宏骥,刘坤,郭猜,丁富荣.MeV能量Si~+引起二次离子发射的研究[J].核电子学与探测技术,2012,32(2):141-144,155.
作者姓名:祝兆文  郑涛  侯杰  聂锐  马宏骥  刘坤  郭猜  丁富荣
作者单位:北京大学物理学院核科学与核技术国家重点实验室,北京,100871
基金项目:国家自然科学基金项目,国家基础科学人才培养基金
摘    要:利用北京大学2×1.7 MV串列加速器终端的飞行时间(TOF)谱仪,分别用1.5、2.0和3.0MeV三种能量的初级束Si+轰击样品来研究其二次离子发射现象,使用的样品包括石墨、碳纳米管等。结果表明,采用合理的降噪方法后得到了高信噪比和高时间分辨率的二次离子质谱,实现了全质量范围无遗漏记谱。利用H-C12峰刻度之后,计算得出二次离子各成分的最可能构成及产额,碳纳米管样品表面氢质量含量为8.15%。同时,发现MeV能区二次离子产额与Si+阻止本领之间的关系并非简单的正相关。

关 键 词:二次离子质谱  飞行时间  降噪  碳纳米管

Study of Secondary Ion Emissions Induced by MeV Si +
ZHU Zhao-wen , ZHENG Tao , HOU Jie , NIE Rui , MA Hong-ji , LIU Kun , GUO Cai , DING Fu-rong.Study of Secondary Ion Emissions Induced by MeV Si +[J].Nuclear Electronics & Detection Technology,2012,32(2):141-144,155.
Authors:ZHU Zhao-wen  ZHENG Tao  HOU Jie  NIE Rui  MA Hong-ji  LIU Kun  GUO Cai  DING Fu-rong
Affiliation:(State Key Laboratory of Nuclear Physics and Technology,School of Physics, Peking University,Beijing 100871,China)
Abstract:Si+ beams of 1.5MeV,2.0MeV and 3.0MeV were used to investigate the secondary ion emission of the samples,such as graphite,carbon nanotubes(CNT) etc,using the accelerator-based time of flight(TOF) SIMS in the Laboratory of 2×1.7 MV tandem accelerator in Peking University.Compared with the previous data,the spectrum was much clearer attribute to the improvement of the noise reduction and the increase of the flight distance.The spectrums were calibrated using the H and C12 peaks,which showed the mass of hydrogen on the surface of CNT reaches 8.15%.The components and products of the secondary ions were precisely calculated and the products were found to be not positively related with the stopping powder of Si+ in the samples.
Keywords:SIMS  TOF  Noise reduction  Carbon nanotube
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