| 电致发光材料9,10-二(6-叔丁基-2-萘基)蒽的合成和纯度分析 |
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| 引用本文： | 吴边鹏,许建华,杨淑英,冯勇刚.电致发光材料9,10-二(6-叔丁基-2-萘基)蒽的合成和纯度分析[J].天津城市建设学院学报,2005,11(4):291-293,297. |
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| 作者姓名： | 吴边鹏 许建华 杨淑英 冯勇刚 |
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| 作者单位： | 天津城市建设学院,材料科学与工程系,天津,300384 |
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| 摘 要： | 9，10-二（6-叔丁基-2-萘基）蒽是一种性能优良的小分子电致发光材料，具有熔点高，热稳定性好，发光效率高的特点．采用格氏反应VA蒽醌和6-溴-2-叔丁基萘为起始原料，合成了该化合物，并通过荧光分光光度法对产品纯度进行了定量分析．批量制备中，仅以重结晶方法进行处理，产品纯度可达到96％以上．
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| 关 键 词： | 9，10-二取代蒽 有机电致发光 荧光染料 格氏反应 |
| 文章编号： | 1006-6853（2005）04-0291-03 |
| 收稿时间： | 2005-06-09 |
| 修稿时间： | 2005-08-30 |
Synthesis and quantitative analysis of compound of 9,10-bis(6-t-butyl-2-naphthyl) anthenace by Grinard reaction |
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| WU Bian-pengI,XU Jian-hua,YANG Shu-ying,FENG Yong-gang.Synthesis and quantitative analysis of compound of 9,10-bis(6-t-butyl-2-naphthyl) anthenace by Grinard reaction[J].Journal of Tianjin Institute of Urban Construction,2005,11(4):291-293,297. |
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| Authors: | WU Bian-pengI XU Jian-hua YANG Shu-ying FENG Yong-gang |
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| Abstract: | 9,10-bis(6-t-butyl-2-naphthyl) anthracene is an organic molecular electroluminescent material with high melt pomt, excellent thermostability and high luminescent efficiency. The compound is sythesized by Grinard Reaction with 6-bromo-2-t-butyl naphthalene and anthraquinone as initiated materials. The quantitative analysis of this compound is made by fluoroscopic method. The purity can be at least 96% only by recrystallization process in scale sythesis. |
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| Keywords: | 9 10-diphenyl anthracene organic electroluminescence fluorescent dye Grinard reaction |
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