溴化N—(3—长链烷氧—2—羟)丙基—N,N,N—三甲基铵的合成及性质 |
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引用本文: | 张广友,赵淑英.溴化N—(3—长链烷氧—2—羟)丙基—N,N,N—三甲基铵的合成及性质[J].表面活性剂工业,1997(2):15-17,20. |
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作者姓名: | 张广友 赵淑英 |
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作者单位: | 山东建材学院应用化学系!济南市,250022 |
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摘 要: | 脂肪醇和环氧氯丙烷在相转移条件下反应得到长链烷基缩水甘油醚,以此为原料和三甲胺氢溴酸盐反应得到溴化N-(3-长链烷氧-2-羟)丙基-N,N,N-三甲基铵。其结构通过红外光谱,核磁共振氢谱及元素分析结果得以证实。本文还测定所合成产品的表面张力和临界胶束浓度等。
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关 键 词: | 脂肪醇 表面活性剂 季铵盐 溴化 阳离子型 |
Synthesis of N-(3-Long Chain Alkyloxy-2-Hydroxy)Propyl-N,N,N,-Trimethylammonium Bromide and Their Properties |
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Authors: | Zhang guangyou |
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Affiliation: | Zhang guangyou et al |
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Abstract: | N-(3-long chain alkyloxy- 2 - hydroxy ) propyl-N, N, N-trimethyl ammonium bromide were synthesized from the reaction of trimethyl ammonium bromide and long chain alkyl glycidyl ether which were prepared from fatty alcohol and epichlorohydrim under a condition of phase transfer catalyst in a yield of 97%.Their structures were confirmed by IR,HNMR and elemental analyses. Surface tension and critical micelle concentration of the products were also determined in this paper. |
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Keywords: | fatty alcohol surfactant quaternary ammonium |
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