| 微波辐射对甲苯磺酸催化合成肉桂酸异丁酯 |
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| 引用本文： | 樊靓,李淑琴.微波辐射对甲苯磺酸催化合成肉桂酸异丁酯[J].云南化工,2006,33(6):25-27. |
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| 作者姓名： | 樊靓 李淑琴 |
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| 作者单位： | 襄樊学院化学与生物科学系,湖北,襄樊,441053 |
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| 摘 要： | 研究了在微波辐射下,用对甲苯磺酸作催化剂,快速合成肉桂酸异丁酯,探讨了影响反应的相关因素。最佳反应条件为:微波功率465 W,催化剂0.45 g,微波辐射时间为9 m in,醇酸的量比为1∶8,转化率可达到94.2%。
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| 关 键 词： | 微波辐射 对甲苯磺酸 肉桂酸异丁酯 催化 |
| 文章编号： | 1004-275X（2006）06-0025-03 |
| 收稿时间： | 2006-06-22 |
| 修稿时间： | 2006-06-22 |
Synthesis of Isobutyl Cinnamate by the Catalysis of p-Toluene Sulphonic Acid under Microwave Radiation |
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| FAN Jing,LI Shu-qing.Synthesis of Isobutyl Cinnamate by the Catalysis of p-Toluene Sulphonic Acid under Microwave Radiation[J].Yunnan Chemical Technology,2006,33(6):25-27. |
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| Authors: | FAN Jing LI Shu-qing |
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| Affiliation: | Department of Chemistry and Biology, Xiangfan School, Xiangfan441053, China |
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| Abstract: | Isobutyl cinnamate was synthesized by the catalysis of p-toluene sulphonic acid under microwave radiation.Effects on the reaction such as amount of catalyst,microwave power,radiation time and molar ratio of alcohol to acid were studied,and the optimal condition was chosen as follows:microwave power of 465W,molar ratio of alcohol to acid of 10∶1,catalyst amount of 0.45g,irradiation time of 9min,with the yield of 94.2%. |
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| Keywords: | microwave radiation p-toluene sulphonic acid isobutyl cinnamate catalyzation |
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