| 对溴苄基乙酰氨基丙二酸二乙酯的合成研究 |
| |
| 引用本文： | 樊劲达 倪家宝. 对溴苄基乙酰氨基丙二酸二乙酯的合成研究[J]. 精细石油化工, 1999, 0(6): 19-21 |
| |
| 作者姓名： | 樊劲达 倪家宝 |
| |
| 作者单位： | 华东理工大学精细化工系!上海，200237，华东理工大学精细化工系!上海，200237，华东理工大学精细化工系!上海，200237 |
| |
| 摘 要： | 通过对溴甲苯溴化合成了对溴苄溴 ( ) ,收率为 4 5.3 % ,从丙二酸二乙酯出发合成了乙酰氨基丙二酸二乙酯 ( ) ,收率为 60 .6% , 和 缩合得到了对溴苄基乙酰氨基丙二酸二乙酯 ,收率为 61 .3 %。
|
| 关 键 词： | 对溴苄溴 乙酰氨基丙二酸二乙酯 缩合 对溴苄基乙酰氨基丙二酸二乙酯 |
THE SYNTHESIS OF DIETHYL P-BROMOBENZYLACETAMIDOMALONATE |
| |
| Fan Jinda,Ni Jiabao and Xian Meiming. THE SYNTHESIS OF DIETHYL P-BROMOBENZYLACETAMIDOMALONATE[J]. Speciality Petrochemicals, 1999, 0(6): 19-21 |
| |
| Authors: | Fan Jinda Ni Jiabao Xian Meiming |
| |
| Abstract: | pBromobenzyl bromide (Ⅰ) was synthesized by bromization of pbromotoluene, diethyl acetamidomalonate (Ⅱ) was prepared from diethyl malonate, the yields were 45.3% and 60.6% respectively; through the condensation of Ⅰ and Ⅱ, the vital intermediate diethyl pbromobenzylacetamidomalonate was obtained, the yield was 61.3%. |
| |
| Keywords: | p-bromobenzyl bromide diethyl acetamidomalonate condensation diethyl pbromobenzylacetamidomalonate |
| 本文献已被 CNKI 维普 等数据库收录！ |
