| 间溴苯甲醚合成工艺的研究 |
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| 引用本文： | 高建荣,何玲辉.间溴苯甲醚合成工艺的研究[J].精细石油化工,1999(6):17-19. |
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| 作者姓名： | 高建荣 何玲辉 |
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| 作者单位： | 浙江工业大学化工学院!杭州，310012，浙江工业大学化工学院!杭州，310012，浙江工业大学化工学院!杭州，310012，浙江工业大学化工学院!杭州，310012 |
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| 摘 要： | 根据反应机理和合成工艺比较 ,研究了以间氨基酚为原料 ,经重氮化、Sandmeyer反应、酸解和醚化合成间溴苯甲醚的工艺过程 ,确定了适宜的工艺参数 ,反应总收率达 53 .3 %。
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| 关 键 词： | 间溴苯甲醚 Sandmeyer反应 重氮化 醚化 |
STUDY ON THE SYNTHESIS PROCESS OF 1-BROMO-3-METHOXYBENZENE |
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| Gao Jianrong,He Linghui,He Xi and Tong Guoton.STUDY ON THE SYNTHESIS PROCESS OF 1-BROMO-3-METHOXYBENZENE[J].Speciality Petrochemicals,1999(6):17-19. |
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| Authors: | Gao Jianrong He Linghui He Xi and Tong Guoton |
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| Abstract: | Based on the principles and the mechanism of reactions, the process for preparation of 1bromo3methoxybenzene by diazotization, Sandmeyer reaction, acid hydrolysis and etherification of maminophenol was studied. The optimal parameters of the process were selected and the yield of the product was 53.3%. |
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| Keywords: | bromo-3-methoxybenzene sandmeyer reaction diazotization etherification |
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