| 6-氨基-7-氟-2H-1,4-苯并(噁)嗪-3(4H)-酮的高效液相色谱法测定 |
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| 引用本文： | 李鹏,杨林. 6-氨基-7-氟-2H-1,4-苯并(噁)嗪-3(4H)-酮的高效液相色谱法测定[J]. 农药, 2006, 45(10) |
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| 作者姓名： | 李鹏 杨林 |
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| 作者单位： | 1. 沈阳工业大学,材料科学与工程学院,沈阳,110023;沈阳化工研究院,沈阳,110021
2. 沈阳工业大学,材料科学与工程学院,沈阳,110023 |
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| 摘 要： | 叙述了采用反向高效液相色谱法,以甲醇为溶剂,甲醇与水(体积比65∶35)为流动相,ODS为填料和紫外检测器分离测定6-氨基-7-氟-2H-1,4-苯并嗪-3(4H)-酮。该方法的标准偏差为0.29,变异系数为0.32%,回收率为99.85%,线性关系系数为0.9997。
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| 关 键 词： | 6-氨基-7-氟-2H-1,4-苯并(噁)嗪-3(4H)-酮 高效液相色谱 分析 |
Determination of 6-amino-7-fluoro-2H-1,4-benzoxazin-3(4H)-one by HPLC |
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| LI Peng,YANG Lin. Determination of 6-amino-7-fluoro-2H-1,4-benzoxazin-3(4H)-one by HPLC[J]. Pesticides, 2006, 45(10) |
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| Authors: | LI Peng YANG Lin |
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| Abstract: | It was introduced that quantitative analysis of 6-amino-7-fluoro-2H-1,4-benzoxazin-3(4H)-one by re-versed phase HPLC,using methanol as solvent,methanol-water(65:35,by vol)as mobile phase,packing by ODS andusing UV detector.The standard deviation was 0.29,coefficient of variation was 0.32%,average recovery was 99.85%,linear correlation was 0.9997. |
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| Keywords: | 6-amino-7-fluoro-2H-1 4-benzoxazin-3(4H)-one HPLC analysis |
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