| 金合欢基丙酮的合成与表征 |
| |
| 引用本文： | 张峻松,贾春晓,毛多斌,张文叶.金合欢基丙酮的合成与表征[J].化学世界,2004,45(2):86-88. |
| |
| 作者姓名： | 张峻松 贾春晓 毛多斌 张文叶 |
| |
| 作者单位： | 郑州轻工业学院食品生物工程系,河南,郑州,450002;郑州轻工业学院食品生物工程系,河南,郑州,450002;郑州轻工业学院食品生物工程系,河南,郑州,450002;郑州轻工业学院食品生物工程系,河南,郑州,450002 |
| |
| 摘 要： | 对合成金合欢基丙酮的工艺路线进行了详细的探讨,确定了以芳樟醇为起始原料,经Car-roll重排反应、格氏反应、催化氢化和Carroll重排反应四步反应的合成路线,合成了金合欢基丙酮,总收率达50.9%。对最终产物进行了红外光谱、核磁共振谱和质谱的测试,证明所得产物为金合欢基丙酮。
|
| 关 键 词： | 芳樟醇 金合欢基丙酮 合成 表征 |
| 文章编号： | 0367-6358(2004)02-0086-03 |
Synthesis and Characterization of Farnesalacetone |
| |
| ZHANG Jun-song,JIA Chun-xiao,MAO Duo-bin,ZHANG Wen-ye.Synthesis and Characterization of Farnesalacetone[J].Chemical World,2004,45(2):86-88. |
| |
| Authors: | ZHANG Jun-song JIA Chun-xiao MAO Duo-bin ZHANG Wen-ye |
| |
| Abstract: | Farnesalacetone was synthesized using linalool as raw material. The process mainly included rearrangement reaction, Grignar reaction, catalytic hydrogenation and rearrangement reaction. The total yield was up to 50.9%. The final product was identified by means of IR spectoscopy, ()~1H NMR spectroscopy and MS, and was proved to be farnesalacetone. |
| |
| Keywords: | linalool farnesalacetone synthesis characterization |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
