| 外源性红花黄色素掺伪葡萄酒鉴别检测方法的研究 |
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| 引用本文： | 刘浩,刘锐萍,杨帛,李志芬,张克义.外源性红花黄色素掺伪葡萄酒鉴别检测方法的研究[J].中国酿造,2014(9):148-150. |
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| 作者姓名： | 刘浩 刘锐萍 杨帛 李志芬 张克义 |
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| 作者单位： | 国家葡萄葡萄酒质量监督检验中心(秦皇岛);秦皇岛市食品药品检验中心; |
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| 基金项目： | 河北省质量技术监督局科技计划项目(2011ZD16) |
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| 摘 要： | 研究了天然色素红花黄掺伪葡萄酒的鉴别检测方法,样品经葡聚糖凝胶提取后用高效液相色谱法测定.确定了红花黄中掺两种主要呈色物质：红花黄A和红花黄B,在10～500mg/L范围内线性关系良好,回收率为85％～93％,相对标准偏差（RSD）＜4％.方法准确、灵敏、简单,适用于葡萄酒中外源红花黄色素的测定.
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| 关 键 词： | 葡萄酒掺伪 鉴别检测 红花黄色素 高效液相色谱法 |
Identification and determination method of exogenous safflor yellow in wine adulteration |
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| Affiliation: | ZHAO Guangxi, LIU Hao, LIU Ruiping, YANG Bo, LI Zhifen, ZHANG Keyi (1.National Center of Supervision ＆ Inspection on Grape and Wine Quality, Qinhuangdao 066000, China; 2.Qinhuangdao Center for Food and Drug Control, Qinhuangdao 066000, China) |
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| Abstract: | The determination of safflor yellow in adulterated wine was developed,in which samples were extracted by sephadex and then determined by HPLC.The main elements of safflor yellow were saffionin A and saffionin B.The calibration curves showed good linearity in the range of 10-500 mg/L,the recovery rate was 85％-93％,and the relative standard deviation was less than 4％.The established method was accurate,sensitive and simple,which was suitable for the exogenous determination of safflor yellow in wine. |
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| Keywords: | grape wine adulteration identification and detection safflor yellow HPLC |
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