Headspace gas analysis of salad oils by mass spectrometry |
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Authors: | C D Evans E Selke |
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Affiliation: | (1) Northern Regional Research Laboratory, 61604 Peoria, Illinois |
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Abstract: | A mass spectrometer was used to analyze the content of hydrogen, nitrogen, oxygen, carbon dioxide and argon in headspace gas
of commercially packaged soybean, cottonseed and corn salad oils. A leakproof sampling system was designed to avoid air contamination
and obtain a representative headspace gas sample. Some edible oils are packaged under pure nitrogen, whereas other samples
contained various amounts of oxygen in the headspace gas. The presence or absence of argon in the headspace gas indicates
that some oils are packaged with pure nitrogen and others with nitrogen obtained by controlled burning of hydrocarbons to
remove all the oxygen in air. The presence of hydrogen in some samples where argon was also present suggested that catalytic
purifiers were used to remove the last traces of oxygen and to ensure pure nitrogen for packaging oils. The decrease in oxygen
of oils bottled in air was followed during storage at room and at elevated temperatures.
No. Market. and Nutr. Res. Div., ARS, USDA. |
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Keywords: | |
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