| 水杨醛缩邻甲苯胺Schiff碱及其Zn(Ⅱ)配合物的合成与表征 |
| |
| 引用本文： | 李轶.水杨醛缩邻甲苯胺Schiff碱及其Zn(Ⅱ)配合物的合成与表征[J].应用化工,2010,39(9). |
| |
| 作者姓名： | 李轶 |
| |
| 作者单位： | 陕西省石油化工研究设计院,陕西,西安,710054 |
| |
| 摘 要： | 由水杨醛和邻甲苯胺缩合形成的不对称Sch iff碱与Zn(Ⅱ)盐反应得到了金属配合物。通过元素分析、红外光谱、紫外-可见光谱、核磁共振氢谱(1H NMR)及13C谱(13C NMR)等分析测试手段对配体及其配合物进行了结构表征,确定了配合物的可能结构,结果表明,配体通过N,O原子与金属离子配位。
|
| 关 键 词： | Schiff碱 配合物 合成与表征 |
Synthesis and characterization of Zn(II) complex derived from salicylaldehycle and o-toluidine |
| |
| LI Yi.Synthesis and characterization of Zn(II) complex derived from salicylaldehycle and o-toluidine[J].Applied chemical industry,2010,39(9). |
| |
| Authors: | LI Yi |
| |
| Abstract: | A Schiff base derived from salicylaldehycle and o-toluidine and its complex of Zn(Ⅱ) were synthesized.The ligand and its complexe were characterized by IR spectra,UV-visible spectra,1H NMR,13C NMR and TG-DTA analysis.The possible structure of the complexs was proposed and it is possible to conclude that the ligand is attached to the metal ion by oxygen and nitrogen atoms. |
| |
| Keywords: | Schiff base complex synthesis and characterization |
| 本文献已被 万方数据 等数据库收录！ |
