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Sol-Gel法制备纳米Fe-TiO_2光催化剂及其光催化性能
引用本文:曾翎,尹炳龙,干均江,姜华昌,杨瑞芹. Sol-Gel法制备纳米Fe-TiO_2光催化剂及其光催化性能[J]. 稀有金属材料与工程, 2010, 0(Z2)
作者姓名:曾翎  尹炳龙  干均江  姜华昌  杨瑞芹
作者单位:浙江科技学院;
基金项目:浙江省自然科学基金项目(Y405139)资助
摘    要:以钛酸四正丁酯和无水乙醇为主要原料,掺杂一定比例的Fe3+,采用溶胶-凝胶法(Sol-Gel)制备TiO2-Fe2O3复合催化剂,并用XRD和SEM等手段进行表征。以4-(2-吡啶偶氮)间苯二酚(PAR)光催化降解为模型反应,在可见光条件下对所制备的催化剂催化性能进行表征和评价。结果表明:掺铁TiO2比不掺杂TiO2有更高的催化活性,同时也验证掺铁量在0.5%时,光催化活性最高。焙烧温度在400℃时,催化活性大。

关 键 词:溶胶-凝胶  二氧化钛  氧化铁  锐钛矿  降解  

Preparation of Nanometer TiO_2-Fe Catalyst by Sol-Gel Method and Its Photocatalytic Performance
Zeng Ling,Yin Binglong,Gan Junjiang,Jiang Huachang,Yang Ruiqin. Preparation of Nanometer TiO_2-Fe Catalyst by Sol-Gel Method and Its Photocatalytic Performance[J]. Rare Metal Materials and Engineering, 2010, 0(Z2)
Authors:Zeng Ling  Yin Binglong  Gan Junjiang  Jiang Huachang  Yang Ruiqin
Affiliation:Zeng Ling,Yin Binglong,Gan Junjiang,Jiang Huachang,Yang Ruiqin (zhejiang University of Science , Technology,Hangzhou 310023,China)
Abstract:Nanometer TiO2-Fe photo catalyst was prepared from Ti (Obu)4, C2H5OH with certain proportion of Fe3+ by sol-gel. The structure of the catalyst were characterized by means of XRD and TEM techniques. The catalytic activity was evaluated by photocatalytic degradation of PAR as a model reaction. The results indicate that the photocatalytic activity of the TiO2-Fe2O3 composite catalyst is improved greatly compared with TiO2, and 0.5%Fe3+ addition leads to the highest photo catalytic activity. It is also high whe...
Keywords:sol-gel  TiO2-Fe  PAR  anatase  degradation  
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