Electron backscattered diffraction study on superplastic properties of coarse-grained Fe-27 at% Al |
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Affiliation: | 1. Department of Neurosurgery, First Affiliated Hospital of China Medical University, Shenyang 110001, PR China;2. Department of Histology and Embryology, College of Basic Medicine, Shenyang Medical College, Shenyang 110034, PR China;3. Department of Immunology, School of Basic Medical Science, China Medical University, Shenyang 110122, PR China;4. Department of Gynecology, First Affiliated Hospital of China Medical University, Shenyang 110001, PR China;1. Department of Engineering Mechanics, School of Mechanics and Civil Engineering, China University of Mining and Technology, Xu Zhou 221116, China;2. Department of Astronautic Science and Mechanics, Harbin Institute of Technology, Harbin 150001, China |
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Abstract: | An electron backscattered diffraction technique has been used to investigate crystallographic features of a superplastic coarse-grained Fe-27 at% Al alloy. Alloy samples studied have been tensile tested in a temperature range between 600 and 800°C in air under an initial strain rate of 1×10−4 s−1. As a result of dynamic recovery and recrystallization, the grain structure undergoes four major transitions: subgrain-boundary formation, grain-boundary migration, formation and growth of recrystallized grains. A model based on the microstructural evolution is described. Subgrains form during an initial stage of high-temperature deformation when deformation is conducted at low temperature (600°C). Upon further deformation at 700°C, grain boundaries migrate, resulting in the formation of new grains. When deformation is made further to a larger elongation or at even higher temperature (800°C), dynamic recovery and recrystallization occur significantly, resulting in grain refinement and hence superplasticity. Refined grains thus formed maintain crystallographic relationships with parent grains. |
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