| 三元乙丙橡胶的1H-NMR定量分析 |
| |
| 引用本文： | 王秀萍,王博,张欣荣.三元乙丙橡胶的1H-NMR定量分析[J].化工科技,2013(6):45-47,51. |
| |
| 作者姓名： | 王秀萍 王博 张欣荣 |
| |
| 作者单位： | [1]中国石油吉林石化公司研究院,吉林吉林132021 [2]中国石油吉林石化公司有机合成厂,吉林吉林132021 |
| |
| 摘 要： | 用核磁共振氢谱法（1 H-NMR）对三元乙丙橡胶进行了研究,通过图谱中各个峰的积分值,并用特定的计算公式测定了三元乙丙橡胶中C2、C3及第三单体乙叉降冰片烯（ENB）的含量,以期为红外光谱（IR）的定量分析提供参考校准数据.
|
| 关 键 词： | 三元乙丙橡胶 C2 C3 ENB 乙叉降冰片烯 1H-NMR |
Quantitative analysis of ethylene-propylene-diene rubber by 1H-NMR spectrometry |
| |
| Wang Xiuping,Wang Bo,Zhang Xinrong.Quantitative analysis of ethylene-propylene-diene rubber by 1H-NMR spectrometry[J].Science & Technology In Chemical Industry,2013(6):45-47,51. |
| |
| Authors: | Wang Xiuping Wang Bo Zhang Xinrong |
| |
| Affiliation: | 1. Research Institute of Jilin Petrochemical Company, PetroChina, Jilin 132021, China 2. Organic Synthesis Factory of J ilin Petrochemical Company, PetroChina , J ilin 132021, China) |
| |
| Abstract: | Components of ethylene-propylene-diene rubber （EPDR） were quantitatively analyzed by 1 H nuclear magnetic resonance spectrometry. The contents of C2, C3 and 5-ethylidene-2-norbornene in several samples of EPDR were determined using a calculation method through the integral areas of peaks. The results of this work could be used for calibration of quantitative analysis in a large scale by infrared spectrometry. |
| |
| Keywords: | Ethylene-propylene-diene rubbers C2 C3 ENB 5-Ethylidene-2-norbornene 1 H-NMR |
| 本文献已被 维普 等数据库收录！ |
