Particle Impact Damage in Silicon Nitride |
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Authors: | Donald A. Shockey,David J. Rowcliffe, ,Kim C. Dao,&dagger ,Lynn Seaman |
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Affiliation: | SRI International, Menlo Park, California 94025-3493 |
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Abstract: | The evolution of particle-impact-induced fracture damage in hot-pressed (HP) silicon nitride was established by accelerating single 2.4-mm-diameter tungsten carbide spheres against polished HP Si3N4 surfaces. Threshold velocities for ring, cone, and radial cracks were determined and the corresponding threshold stress for ring cracking was obtained from an elastic stress analysis. Particle size had significant effects on the threshold velocities for the inelastic impression and the various crack types. Loading rate had little effect on the threshold stress for ring cracks; rate effects on other crack types could not be assessed because the quasistatic indenter failed at stresses less than those required to invoke other crack types. A 20-μm-thick oxide scale had little influence on morphology and extent of damage but was removed easily at low velocities, suggesting higher erosion rates for Si3N4 in oxidizing environments. Damage phenomenology in 85% dense reaction-bonded Si3N4 was similar to that in HP material; however, all stages of damage occurred at substantially lower velocities. |
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Keywords: | silicon nitride impact cracks damage hot pressing |
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