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光固化ZrO2陶瓷料浆的流变性能研究
引用本文:韩卓群,李伶,刘时浩,邱坤,王守兴,刘福田. 光固化ZrO2陶瓷料浆的流变性能研究[J]. 硅酸盐通报, 2021, 40(6): 1965-1971
作者姓名:韩卓群  李伶  刘时浩  邱坤  王守兴  刘福田
作者单位:济南大学材料科学与工程学院,济南 250022;山东工业陶瓷研究设计院有限公司,淄博 255000
基金项目:国家重点研发计划(2017YFB0310400);山东省重大科技创新工程项目(2019JZZY010440)
摘    要:围绕陶瓷粉体在光敏树脂中的分散,研究了粉体性质、分散剂种类及其掺加量、固含量对光固化ZrO2陶瓷料浆流变性能的影响.结果表明:粉体性质对料浆的流变性能有着显著影响,比表面积小、球形度高的ZrO2陶瓷粉体更有利于配制低粘度、高固含量的料浆;料浆的流变性能以及稳定性主要受分散剂种类及其掺加量的控制,以相对粉体质量4%的X-...

关 键 词:ZrO2陶瓷  光固化  料浆  成型  流变性能
收稿时间:2021-03-22

Research on Rheological Properties of Stereolithography ZrO2 Ceramic Slurry
HAN Zhuoqun,LI Ling,LIU Shihao,QIU Kun,WANG Shouxing,LIU Futian. Research on Rheological Properties of Stereolithography ZrO2 Ceramic Slurry[J]. Bulletin of the Chinese Ceramic Society, 2021, 40(6): 1965-1971
Authors:HAN Zhuoqun  LI Ling  LIU Shihao  QIU Kun  WANG Shouxing  LIU Futian
Affiliation:1. School of Materials Science and Engineering, University of Jinan, Jinan 250022, China; 2. Shandong Industrial Ceramics Research & Design Institute Co., Ltd., Zibo 255000, China
Abstract:This paper focuses on the dispersion of ceramic powder in photosensitive resin. The effects of powder properties, dispersant type and dosage, and solid content on the rheological properties of stereolithography ZrO2 ceramic slurry were studied. The result shows that the properties of the powder have a significant impact on the rheological properties of the slurry, the use of ZrO2 powder with a smaller specific surface area and higher sphericity is more conducive to the preparation of low viscosity and high solid content slurry. The rheological properties and stability of the slurry are mainly controlled by the type and dosage of dispersant, using X-100 with a relative powder mass of 4% as a dispersant, the rheological properties and stability of the prepared ceramic slurry are better. The experimental result of the solid content of the slurry shows that the relationship between the solid content of the slurry and the viscosity satisfies the Krieger-Dougherty model. And the dispersion mechanism of the dispersant has been studied. By the research of this experiment, the foundation has been laid for the high-precision molding of the light-cured ZrO2 ceramic slurry.
Keywords:ZrO2 ceramic  stereolithography  slurry  molding  rheological property  
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