| 1，3－二氯－2－丁烯氯化产物的气相色谱分析 |
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| 引用本文： | 江朝学,王成名. 1，3－二氯－2－丁烯氯化产物的气相色谱分析[J]. 合成橡胶工业, 1994, 0(1) |
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| 作者姓名： | 江朝学 王成名 |
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| 作者单位： | 长寿化工总厂 |
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| 摘 要： | 用气相色谱法测定１，３－二氯－２－丁烯的氯化产物，采用３０１釉化担体：阿皮松Ｌ：聚乙二醇－２０Ｍ－２－硝基对苯二甲酸＝１００：１０：０．８（质量比）的固定相填充柱分离了氯化产物中１６个组分。用色谱－质谱联用法鉴定这些组分为２，３，４－三氯－１－丁烯、２－甲基－３，３，３－三氯－１－丙烯、１，２，３，３－四氯丁烷、１，２，３，３，４－五氯丁烷等。用面积归一化法计算出了氯化产物中各组分含量。
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| 关 键 词： | 1，3－二氯－2－丁烯，色谱－质谱法，核磁共振波谱法，定性分析，定量分析 |
GAS CHROMATOGRAPHY ANALYSIS OF 1, 3-DICHLORO -2-BUTENE CHLORINATE |
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| Jiang Chaoxue and Wang Chengming. GAS CHROMATOGRAPHY ANALYSIS OF 1, 3-DICHLORO -2-BUTENE CHLORINATE[J]. China Synthetic Rubber Industry, 1994, 0(1) |
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| Authors: | Jiang Chaoxue and Wang Chengming |
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| Abstract: | The chlorinate of 1,3-dichloro-2-butene (DCB)was determined by gas chromatography. Sixteen components in the chlorinate were separated by a column packed with 301-glazed supporter: Apiezon-L: FFAP of 100:10:0.8 (mass ratio). The components were identified by gas chromatograph-mass spectrometer.The composition of chlorinate of DCB was determined by the area normalization method. |
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| Keywords: | dichloro-2-butene gas chromatograph-mass spectrometer muclear magnetic resonance spectroscopy qualitative analysis quantitative analysis |
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