| 灌冠红梅子挥发性化学成分的GC/MS分析 |
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| 引用本文： | 宋京都,杨婕,李华民,文永奇,裴强,何兰.灌冠红梅子挥发性化学成分的GC/MS分析[J].质谱学报,2006,27(2):110-112. |
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| 作者姓名： | 宋京都 杨婕 李华民 文永奇 裴强 何兰 |
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| 作者单位： | 1.甘肃省药检所,甘肃 兰州 730000;
2.北京师范大学化学系，北京 100875 |
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| 摘 要： | 将灌冠红梅子根的乙醇提取物用甲醇溶解，加水，用石油醚萃取，采用GC/MS法进行分析。以峰面积归一化法计算各化合物在挥发油中的相对含量，共鉴定出个22化学成分，占总体含量的 98.32%。主要成分有4-甲基-2-乙基己烷（14.79%）、反式-1-甲氧基-1-丁烯（13.41%）、2,3,3-三甲基己烷（10.24%）、(1-甲氧基-1-戊基)环丙烷（10.22%）、N,N-二甲基叔丁基胺(9.23%)、环己烷（8.55%）、1,1-二甲氧基-2-丁炔（6.34%）、2-甲基-2-乙基环氧乙烷（6.25%）、庚烷（4.38%）、正十一烷（3.6%）、1-碘正十四烷（2.6%）。
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| 关 键 词： | 灌冠红梅子 化学成分 GC/MS |
| 文章编号： | 1004-2997（2006）02-110-03 |
| 收稿时间： | 2005-08-04 |
| 修稿时间： | 2005-11-07 |
Analysis of Essential Constituents from Rubus xanthocarpus by GC/MS |
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| SONG Jing-du,YANG Jie,LI Hua-min,WEN Yong-qi,PEI Qiang,HE Lan.Analysis of Essential Constituents from Rubus xanthocarpus by GC/MS[J].Journal of Chinese Mass Spectrometry Society,2006,27(2):110-112. |
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| Authors: | SONG Jing-du YANG Jie LI Hua-min WEN Yong-qi PEI Qiang HE Lan |
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| Affiliation: | 1. Gansu Provincial Institute for Drug Control, Lanzhou 730000, China;
2. Deptment of Chemistry, Beijing Normal University, Beijing 100875, China |
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| Abstract: | Root of Rubus xanthocarpus was extracted with ethanol,followed by methanol dissolving.Then water was added to the methanol solution,and extracted by petrolic ether.The essential chemical components from Rubus xanthocarpus were analyzed by GC/MS.Twenty-two components from Rubus xanthocarpus were identified by library search,which accounted for over 98.32% of total volatile components.The main components are 4-methyl-2-ethylhexane(14.79%),trans-1-methoxy-1-butene(13.41%),2,3,3-trimethylhexane (10.24%),(1-methoxy-1-pentyl)cyclopropane(10.22%),N,N-dimethylt-butylamine(9.23%),cyclohexane(8.55%),1,1-dimethoxy-2-butyne(6.34%),2-methyl-2-ethyl ethylene oxide(6.25%),heptane(4.38%),n-undecane(3.6%),1-iodoteradecane(2.6%). |
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| Keywords: | GC/MS |
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