| 同时蒸馏萃取技术分析酿酒原料青稞中挥发性化合物的研究 |
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| 引用本文： | 张晓磊 ,,李春扬 ,张世满 ,安红梅 ,杨兴华 ,尹建军 ,宋全厚 .同时蒸馏萃取技术分析酿酒原料青稞中挥发性化合物的研究[J].酿酒科技,2012(7):115-118,123. |
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| 作者姓名： | 张晓磊 李春扬 张世满 安红梅 杨兴华 尹建军 宋全厚 |
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| 作者单位： | （1.中国食品发酵工业研究院，北京 100027;2.国家食品质量监督检验中心，北京 100027;3.青海互助青稞酒有限公司，青海 互助 810500） |
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| 摘 要： | 建立了同时蒸馏萃取-气相色谱/质谱联用技术（SDE-GC/MS）分析青稞中挥发性化合物的方法，获得 26 种组分的定性和定量结果。采用这一技术对瓦蓝、肚里黄、白青稞、黑老鸭等四种青稞酒原料进行分析，结果表明不同青稞品种间化合物种类接近又各具特点。本研究还对同时蒸馏萃取技术参数优化、青稞中主要挥发性组分进行了分析研究。
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| 关 键 词： | 同时蒸馏萃取 气相色谱/质谱 酿酒原料 青稞 挥发性化合物 |
Analysis of Volatile Compounds in Hullessbarley by Simultaneous Distillation and Extraction Coupled with GC-MS |
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| ZHANG Xiaolei,LI Chunyang,ZHANG Shiman,AN Hongmei,YANG Xinghua,YIN Jianjun,and SONG Quanhou.Analysis of Volatile Compounds in Hullessbarley by Simultaneous Distillation and Extraction Coupled with GC-MS[J].Liquor-making Science & Technology,2012(7):115-118,123. |
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| Authors: | ZHANG Xiaolei LI Chunyang ZHANG Shiman AN Hongmei YANG Xinghua YIN Jianjun and SONG Quanhou |
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| Affiliation: | 1,2(1.China National Research Institute of Food and Fermentation Industries,Beijing 100027;2.National Center for Food Quality Supervision and Testing,Beijing 100027;3.Qinghai Huzhu Highland Barley Wine Co.Ltd.,Huzhu,Qinghai 810500,China) |
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| Abstract: | The analysis of volatile compounds in hullessbarley by simultaneous distillation and extraction(SDE) coupled with gas chromatogra-phy-mass spectrometry(GC/MS) had been developed.Four kinds of materials of highland barley liquor including Walan,Dulihuang,Baiqingke and Heilaoya were analyzed by used of such technolgy.Therefore,26 kinds of volatile compounds were identified.The results showed that hul-lessbarley of different types had similar components but each had its individual characteristics.Besides,the optimization of technical parameters of SDE was carried out in this study. |
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| Keywords: | simultaneous distillation and extraction gas chromatography-mass spectrometry liquor-making materials hullessbarley volatile compounds |
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