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Fe-Co薄膜与Al2O3 基体相互扩散和相互作用相关的微观结构演变
引用本文:李致朋,区定容,叶飞.Fe-Co薄膜与Al2O3 基体相互扩散和相互作用相关的微观结构演变[J].稀有金属材料与工程,2021,50(5):1556-1562.
作者姓名:李致朋  区定容  叶飞
作者单位:Zynergy Technology Incorporation, USA Fremont 94538,南方科技大学 材料科学与工程系,广东 深圳 518055,南方科技大学 材料科学与工程系,广东 深圳 518055
摘    要:利用先进分析透射电子显微镜,检测并系统地研究了磁控溅射Fe-Co薄膜与Al2O3基体之间的相互扩散。结果表明,扩散会形成尖晶石相FeAl2O4,并导致界面层的形成。微观结构表征表明,在界面附近的Fe-Co薄膜中形成了与相互扩散相关的非公度结构。本研究不仅检测到Fe-Co薄膜与蓝宝石基体之间的相互扩散和伴随的新相形成,而且揭示了界面区域相应的微观结构演变,这些结果可能对薄膜的磁学性质有很大的影响。

关 键 词:Fe-Co合金  相互扩散  界面  微观结构  透射电子显微镜
收稿时间:2020/2/15 0:00:00
修稿时间:2020/2/22 0:00:00

Interdiffusion and Interaction Associated Microstructure Evolution Between Fe-Co Thin Film and Al2O3 Substrate
Li Zhipeng,Ou Dingrong and Ye Fei.Interdiffusion and Interaction Associated Microstructure Evolution Between Fe-Co Thin Film and Al2O3 Substrate[J].Rare Metal Materials and Engineering,2021,50(5):1556-1562.
Authors:Li Zhipeng  Ou Dingrong and Ye Fei
Affiliation:Zynergy Technology Incorporation, Fremont 94538, USA,Materials Science and Engineering, Southern University of Science and Technology, Shenzhen 518055, China,Materials Science and Engineering, Southern University of Science and Technology, Shenzhen 518055, China
Abstract:By advanced analytical transmission electron microscope, an unexpected interdiffusion between magnetron sputtered Fe-Co thin film and Al2O3 substrate was detected and systematically investigated in this study. Results show that a new phase of spinel FeAl2O4 forms, leading to the formation of interfacial layer. Detailed microstructure characterization reveals the interdiffusion associated with incommensurate structure formation near the interface in the Fe-Co thin film. The interdiffusion and accompanied new phase formation between the Fe-Co thin film and sapphire substrate are detected, and the associated microstructure evolution at the interfacial region is discussed, which may considerably influence the thin film magnetic properties.
Keywords:Fe-Co alloy  interdiffusion  interface  microstructure  transmission electron microscope
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