| 以L胱氨酸为硫源的溶剂热方法生长Sb_2S_3纳米带(英文) |
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| 引用本文： | 杨昕宇,钟家松,刘丽君,梁晓娟,刘海涛,向卫东.以L胱氨酸为硫源的溶剂热方法生长Sb_2S_3纳米带(英文)[J].稀有金属材料与工程,2010(Z2). |
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| 作者姓名： | 杨昕宇 钟家松 刘丽君 梁晓娟 刘海涛 向卫东 |
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| 作者单位： | 温州大学; |
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| 基金项目： | National Natural Science Foundation of China (50772075) |
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| 摘 要： | 用L光氨酸作为一种新型硫源,以乙二醇和去离子水的混合溶液作为溶剂在180℃,24h的条件下成功地生长出Sb2S3纳米带。该纳米带长度在十几个微米,宽度在100～300nm。该纳米带为立方结构,通过分析提出了一种合理的生长机理。该纳米带的微观结构通过XRD和FESEM进行了表征。
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| 关 键 词： | 纳米结构 硫化物 化学合成 电子显微镜 |
Solvothermal Growth of Sb_2S_3 Nanoribbons with L-Cystine as Sulfur Source |
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| Yang Xinyu,Zhong Jiasong,Liu Lijun,Liang Xiaojuan,Liu Haitao,Xiang Weidong.Solvothermal Growth of Sb_2S_3 Nanoribbons with L-Cystine as Sulfur Source[J].Rare Metal Materials and Engineering,2010(Z2). |
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| Authors: | Yang Xinyu Zhong Jiasong Liu Lijun Liang Xiaojuan Liu Haitao Xiang Weidong |
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| Affiliation: | Yang Xinyu,Zhong Jiasong,Liu Lijun,Liang Xiaojuan,Liu Haitao,Xiang Weidong (Wenzhou University,Wenzhou 325035,China) |
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| Abstract: | L-Cystine was applied successfully as a novel source of sulfur for Sb2S3 nanoribbons growth at 180 oC for 24 h in a mixed solution made of ethylene glycol and distilled water. The nanoribbons were usually tens of microns in length, typically 100-300 nm in width. The structure of the nanoribbons was determined to be of the orthorhombic. A reasonable mechanism was proposed for the growth of Sb2S3 nanoribbons. The as-obtained Sb2S3 products were examined by various techniques including X-ray powder diffraction... |
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| Keywords: | nanostructures chalcogenides chemical synthesis electron microscopy |
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