| N掺杂介孔TiO2纳米粉体的制备 |
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| 引用本文： | 武利娜,宁青菊,李艳杰. N掺杂介孔TiO2纳米粉体的制备[J]. 化工新型材料, 2009, 37(4) |
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| 作者姓名： | 武利娜 宁青菊 李艳杰 |
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| 作者单位： | 陕西科技大学材料科学与工程学院,西安,710021;陕西科技大学材料科学与工程学院,西安,710021;陕西科技大学材料科学与工程学院,西安,710021 |
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| 摘 要： | 以聚乙二醇400为表面活性剂、二乙醇胺为抑制剂,采用蒸发诱导自组装法(EISA)制备了介孔TiO2纳米粉体,并利用尿素为掺杂剂通过固相反应制备出高活性N掺杂介孔TiO2纳米粉体.利用XRD、FE-SEM、TG-DSC等方法对粉体的物相和形貌进行分析表征.结果表明,合成的粉体尺寸分布均匀、纯度高、具有均匀分布的介孔网状结构;N掺杂使介孔TiO2纳米粉体的UV-Vis光吸收曲线产生红移.
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| 关 键 词： | 介孔TiO2 纳米粉体 N掺杂 |
Preparation of N-doped mesoporous TiO_2 nano-powder |
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| Wu Lina,Ning Qingju,Li Yanjie. Preparation of N-doped mesoporous TiO_2 nano-powder[J]. New Chemical Materials, 2009, 37(4) |
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| Authors: | Wu Lina Ning Qingju Li Yanjie |
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| Affiliation: | School of Materials Science and Engineering;Shaanxi University of Science and Technology;Xi'an 710021 |
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| Abstract: | Mesoporous TiO2 powder was prepared using polyethylene glycol as surfactant and diethanolamine as depressor by evaporation-induced self-assembly(EISA) process.Highly activity N-doped mesoporous TiO2 nano-powder was also prepared using urea as dopant by solid state reaction.The shape composition and morphology of as-prepared powder were characterized by XRD,FE-SEM,TG-DSC,etc.The results showed that the as-prepared powder had uniform particle size distribution,high purity and with mesoporous network.The absor... |
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| Keywords: | mesoporous TiO2 nano-powder N-doping |
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