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等离子体原子发射光谱法间接测定铁红中微量硫酸根的研究
引用本文:徐立.等离子体原子发射光谱法间接测定铁红中微量硫酸根的研究[J].广东有色金属学报,2001,11(1):71-74.
作者姓名:徐立
作者单位:广州有色金属研究院分析检测研究中心 广东广州
摘    要:用一定量的Ba^2 将铁红(Fe2O3)中的SO4^2-以BaSO4形式分离,然后用等离子体光谱法测定余量的Ba^2 ,从而间接测得SO4^2-的含量,该法操作简便、检测快速,相对标准偏差小于9.0%(n=5),加料回收率93.0%-99.3%。

关 键 词:铁红  硫酸根  ICP-AES  测定  颜料

Indirect determination of micro SO_4~(2-) in iron oxide red using inductive coupling plasma atomic emission spectrometry
XU Li.Indirect determination of micro SO_4~(2-) in iron oxide red using inductive coupling plasma atomic emission spectrometry[J].Journal of Guangdong Non-Ferrous Metals,2001,11(1):71-74.
Authors:XU Li
Abstract:In this paper, a method is proposed in which a certain amount of Ba2+ is added into a iron oxide red (Fe2O3) solution so that SO2-4 in it is separated in the form of BaSO4, the ex-tra Ba2+ in the solution is then determined by ICP-AES, thus the content of SO2-4 is indirectly determined. The method is simple in operation, fast in detecting, with the relative stan-dard deviation less than 9. 0% (n=5) and the addition recovery of 93. 0%~99. 3%.
Keywords:ICP-spectrometry  iron oxide red  SO2-4  Ba2+
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