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ICP-AES法测定氟钽酸钾中钙镁含量
引用本文:宋金华.ICP-AES法测定氟钽酸钾中钙镁含量[J].稀有金属与硬质合金,2012,40(1):59-61.
作者姓名:宋金华
作者单位:九江有色金属冶炼有限公司,江西九江,332014
摘    要:采用ICP-AES法测定氟钽酸钾中钙、镁的含量.结果表明,在确定了分析谱线、检出限及测定下限、基体浓度、溶样酸度的条件下,测定样品的钙、镁加标回收率为100.58%~102.50%,钙、镁含量测定的相对标准偏差(RSD)为0.74%~10.02%.该方法准确可靠,操作简便快速,精密度高.

关 键 词:ICP-AES法  氟钽酸钾  钙、镁含量

Determination of Calcium and Magnesium in Potassium Fluotantalate by ICP-AES
SONG Jin-hua.Determination of Calcium and Magnesium in Potassium Fluotantalate by ICP-AES[J].Rare Metals and Cemented Carbides,2012,40(1):59-61.
Authors:SONG Jin-hua
Affiliation:SONG Jin-hua(Jiujiang Tanbre CO.,LTD,Jiujiang 332014,China)
Abstract:The content of Ca and Mg in potassium fluotantalate was determined by ICP-AES.After the conditions are determined of analytical spectral lines,detection limit,determination limit,bulk concentration and dissolving acidity,the Ca and Mg recovery of standard addition is 100.58%~102.50%,and RSD value is 0.74%~10.02% for the measured Ca and Mg content.The method is reliable,simple and fast to operate with high precision.
Keywords:ICP-AES  potassium fluotantalate  Ca and Mg content
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