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1,2,3,5-四甲苯催化制备1,2,4,5-四甲苯反应体系的气相色谱分析
引用本文:李云,陈尔霆,聂英龙. 1,2,3,5-四甲苯催化制备1,2,4,5-四甲苯反应体系的气相色谱分析[J]. 沈阳化工学院学报, 1995, 0(3)
作者姓名:李云  陈尔霆  聂英龙
作者单位:沈阳化工学院精细化工系
摘    要:在聚乙二醇-20M的毛细管柱上建立了1,2,3,5-四甲苯催化制备1,2,4,5-四甲苯反应体系的气相色谱分析方法。采取校正面积归一法定量,测定相对校正因子的变异系数小于2%,组分含量分析的相对误差小于3%。

关 键 词:气相色谱;毛细管柱;变异系数;相对误差

Gas Chromatography Analysis of Reaction System of Preparing 1,2,4,5-Tetramethylbenzene
Li Yun ,Chen Erting, Nie Yinglong. Gas Chromatography Analysis of Reaction System of Preparing 1,2,4,5-Tetramethylbenzene[J]. Journal of Shenyang Institute of Chemical Technolgy, 1995, 0(3)
Authors:Li Yun   Chen Erting   Nie Yinglong
Abstract:The analysis of reaction system,in which 1,2,3,5-tetramethylbenzene was catalytically converted to 1,2,4,5-tetramethylbenzene, was investigated on the glass capillary column covered with polyethylene glycol 20M by gas chromatography.Quantitative determinatlon was carried out by using the corrected area normalization,The variation coefficience of relative correction factors were less than 2 %. The relative errors of the component were less than 3%.
Keywords:gas chromatography  glass capillary column  variation coefficience  relative error
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