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多级喷雾碳化法制备纳米碳酸钙工艺研究
引用本文:徐旺生,何秉忠,金士威,宣爱国.多级喷雾碳化法制备纳米碳酸钙工艺研究[J].无机材料学报,2001,16(5):985-988.
作者姓名:徐旺生  何秉忠  金士威  宣爱国
作者单位:武汉化工学院化工系 武汉 430073
摘    要:研究了多级喷雾碳化法制备纳米碳酸钙的工艺,并详细讨论了雾化、碳化条件及添加剂量等对纳米碳酸钙粒径的影响.碳化后的沉淀物经真空干燥,其原始粒径约为30nm.经表面改性处理,可得到粒径在30~40nm范围的活性纳米碳酸钙粉体材料.

关 键 词:纳米碳酸钙  喷雾碳化  粒径  传质系数  
文章编号:1000-324(2001)05-0985-04
收稿时间:2001-2-7
修稿时间:2001年2月7日

Preparation of Nanometer Calcium Carbonate by Multistage Spray Carbonation
XU Wang-Sheng,HE Bing-Zhong,JIN Shi-Wei,XUAN Ai-Guo.Preparation of Nanometer Calcium Carbonate by Multistage Spray Carbonation[J].Journal of Inorganic Materials,2001,16(5):985-988.
Authors:XU Wang-Sheng  HE Bing-Zhong  JIN Shi-Wei  XUAN Ai-Guo
Affiliation:Dept. of Chem. Eng.; Wuhan Institute of Chemical Technology; Wuhan 430073; China
Abstract:The preparation process of nanometer calcium carbonate(CaCO3) by multistage spray carbonation was studied. The effects of the conditions of spray carbonation and additive dosage on the average particle size of nanometer CaCO3 were discussed systematically. The primary particle size of carbonated sediment was about 30nm by vacuum desiccation. Then the active nanometer CaCO3 particles ranged from 30nm to 40nm were obtained by means of surfaction.
Keywords:nanometer calcium carbonate  multistage spray carbonation  particle size  mass transfer coefficient
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