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超临界CO2提取辣椒油树脂工艺的研究
引用本文:金靓婕,朱世云,梁承红,李荫. 超临界CO2提取辣椒油树脂工艺的研究[J]. 食品工业科技, 2012, 33(5): 185-189
作者姓名:金靓婕  朱世云  梁承红  李荫
作者单位:1. 海军航空工程学院,山东烟台,264001
2. 上海交通大学环境科学与工程学院,上海,200240
基金项目:国家自然科学资助项目(20672030)
摘    要:以红辣椒粉为原料,采用超临界CO2萃取法提取辣椒油树脂。以辣椒油树脂的收率为评价指标,确定最佳工艺条件为:萃取压力25MPa,萃取温度30℃,萃取时间3h,此条件下辣椒油树脂收率为10.09%±0.29%。对比实验结果显示:超临界CO2法所得的辣椒油树脂的色价为303±5,辣椒素质量浓度为3.7%±0.7%,均明显优于传统的索氏提取法。对超临界CO2法所得的辣椒油树脂进行二次超临界萃取,可将辣椒红色素和辣椒素进行初步分离。

关 键 词:超临界CO2萃取法  辣椒油树脂  辣椒红色素  辣椒素

Study on extraction process of capsicum oleoresin by supercritical carbon dioxide
JIN Liang-jie,ZHU Shi-yun,LIANG Cheng-hong,LI Yin. Study on extraction process of capsicum oleoresin by supercritical carbon dioxide[J]. Science and Technology of Food Industry, 2012, 33(5): 185-189
Authors:JIN Liang-jie  ZHU Shi-yun  LIANG Cheng-hong  LI Yin
Affiliation:1(1.Naval Aeronautical and Astronautic University,Yantai 264001,China;2.School of Environmental Science and Engineering,Shanghai Jiaotong University,Shanghai 200240,China)
Abstract:Supercritical carbon dioxide was applied in the extraction of capsicum oleoresin with the red capsicum’s smash as the raw material.With the yield of capsicum oleoresin as an index,the optimal conditions were as follows:pressure(25MPa),temperature(30℃),time(3h),and the extraction rate of capsicum oleoresin up to 10.09%±0.29%.Under the conditions,the color value of the capsicum oleoresin extracted by supercritical carbon dioxide was 303±5 and the mass concentration of capsaicin was 3.7%±0.7%,obviously better than that from soxhlet extraction.With the capsicum oleoresin extracted by supercritical carbon dioxide as the material,the capsicum red pigment and the capsaicin could be primarily separated by another supercritical carbon dioxide extraction.
Keywords:supercritical carbon dioxide  capsicum oleoresin  pigment  capsaicin
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