Preparation of Highly Oriented Aluminum Nitride Thin Films on Polycrystalline Substrates by Helicon Plasma Sputtering and Annealing |
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Authors: | Morito Akiyama Chao-Nan Xu Masaya Kodama Ichiro Usui Kazuhiro Nonaka Tadahiko Watanabe |
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Affiliation: | Department of Inorganic Composite Materials, Kyushu National Industrial Research Institute, Tosu, Saga 841–0052 Japan;and Yaemizo, Saga 849–0932 Japan;Industrial Technology Center of Saga, Yaemizo, Saga 849–0932 Japan |
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Abstract: | Highly c -axis-oriented aluminum nitride (AlN) thin films were prepared on polycrystalline Si3N4 and SiC substrates by helicon plasma sputtering. The difference in the substrate materials scarcely influenced the crystal structures of the films. The full width at half-maximum (FWHM) of the X-ray rocking curves of the films was 3.2°, which is the smallest value for AlN thin films deposited on polycrystalline substrates to our knowledge. Annealing at 800°C in vacuum decreased the FWHM from 3.2° to 2.8°. The structure of the films was densely packed and consisted of many fibrous grains. The films developed c -axis orientation on the polycrystalline substrates, because the interaction between the films and substrate surfaces was small, and (100) and (110) AlN planes grew preferentially. The films were piezoelectric and generated electrical signals in response to mechanical stress. |
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Keywords: | aluminum nitride orientation annealing |
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