| 高纯8-羟基喹啉铝的简便合成方法 |
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| 引用本文： | 朱凌健,郭灿城.高纯8-羟基喹啉铝的简便合成方法[J].化学试剂,2004,26(6):369-370. |
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| 作者姓名： | 朱凌健 郭灿城 |
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| 作者单位： | 湖南大学,化学化工学院,湖南,长沙,410082;湖南大学,化学化工学院,湖南,长沙,410082 |
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| 基金项目： | 国家自然科学基金资助 (2 0 3 760 18，2 0 43 60 10 ) |
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| 摘 要： | 研究了反应体系的酸度和反应时间对产物8-羟基喹啉铝(Alq3)纯度及产率的影响，用改进了的方法制备出了高纯度有机电致发光材料Alq3，通过NMR、MS和UV-Vis光谱对其结构进行了表征，并用液相色谱对其纯度进行了检测。
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| 关 键 词： | Alq3 制备 方法改进 |
| 文章编号： | 0258-3283(2004)06-0369-02 |
An improved method for preparation of high-purity tris-(8-hydroxyquinoling )aluminum |
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| ZHU Ling-jian,GUO Can-Cheng.An improved method for preparation of high-purity tris-(8-hydroxyquinoling )aluminum[J].Chemical Reagents,2004,26(6):369-370. |
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| Authors: | ZHU Ling-jian GUO Can-Cheng |
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| Affiliation: | ZHU Ling-jian,GUO Can-cheng * |
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| Abstract: | We studied the influence of the system acidity and the reaction time on the purity and yields of tris-(8-hydroxyquinoline) aluminum(Alq 3) and prepared high-purity organic electroluminescent material of Alq 3 in an improved method.We testified the structure with NMR,MS and UV-Vis spectra and detected the purity of Alq 3 by liquid chromatography. |
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| Keywords: | Alq 3 preparation improved method |
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