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微波消解/ICP-AES法测定面制食品中五种常量元素的含量
引用本文:覃毅磊,赖毅东,何雪芬. 微波消解/ICP-AES法测定面制食品中五种常量元素的含量[J]. 食品工业科技, 2010, 0(2)
作者姓名:覃毅磊  赖毅东  何雪芬
作者单位:东莞市质量计量监督检测所,广东东莞,523120
摘    要:基于国标法对食物中五种常量元素(Ca、Fe、Na、K、Zn)检测的缺陷,本文探讨了用ICP-AES法测定面制食品中五种常量元素,与国家标准测试方法相比,微波消解/ICP-AES法测定样品更具优势,该方法的线性范围为0.1~30μg/mL,检出限低于0.01μg/mL,RSD小于0.5%。与传统的酸解法样品处理相比,不但分析结果相吻合,而且更具有快速、高效、污染少等优点,完全能满足食品分析的要求。

关 键 词:微波消解  ICP-AES法  面制食品  常量元素  

Determination of five macroelements in flour products by microwave digestion/ICP-AES
QIN Yi-lei,LAI Yi-dong,HE Xue-fen. Determination of five macroelements in flour products by microwave digestion/ICP-AES[J]. Science and Technology of Food Industry, 2010, 0(2)
Authors:QIN Yi-lei  LAI Yi-dong  HE Xue-fen
Affiliation:QIN Yi-lei,LAI Yi-dong,HE Xue-fen(Guangdong Dongguan Supervision Testing Institute of Quality , Metrology,Dongguan 523120,China)
Abstract:Because of the faults of the standard methods of food inspection.the method of ICP-AES have been developed to determine the content of five macroelements(Ca、Fe、Na、K、Zn)in flour products.The method is better than another method of digestion.And its detection limit is below 0.01μg/mL and the linear range is 0.1~30μg/mL.RSD is below0.5%.Compared with the traditional acid digestion method.the ICP-AES method is not only matched to the traditional analysis results,but also has advantages of high-speed,high-efficiency and lowemission.The method can satisfy the requirements of food analysis.
Keywords:microwave digestion  ICP-AES  flour products  macroelement  
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