微乳水热法制备单晶BaCO3纳米线 |
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引用本文: | 邓兆,戴英,陈文.微乳水热法制备单晶BaCO3纳米线[J].纳米科技,2009,6(5):40-44,49. |
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作者姓名: | 邓兆 戴英 陈文 |
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作者单位: | [1]武汉理工大学材料科学与工程学院,湖北武汉430070 [2]武汉理工大学材料复合新技术国家重点实验室,湖北武汉430070 |
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基金项目: | Acknowledgment This work was supported by NSFC (50672072) The financial support is gratefully acknowledged. |
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摘 要: | 利用反相胶束结合溶剂热法制备了BaCO3单晶纳米线。该方法中,油酸/正辛烷/水体系中的反相胶柬起到模板作用,引导BaCO3沿一维方向生长,通过X射线衍射(XRD)、扫描电子显微镜(SEM)、投射电子显微镜(TEM)和高分辨电子显微镜(HRTEM)对BaCO3纳米线进行了表征,结果表明,所制备的BaCO3纳米线为均匀的直线形单晶纳米线,直径为80~200nm,长度为几百纳米到几微米。对BaCO3纳米线的形成机理进行了分析。
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关 键 词: | BaCO3 纳米线 反相胶束 |
Synthesis of Single-crystalline Barium Carbonate Nanowires Through a Reverse Micelle Modified Solvothermal Method |
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Authors: | DENG Zhao DAI Ying CHEN Wen |
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Affiliation: | 1. School of Materials Science and Engineering, Wuhan University of Technology, Wuhan 430070, China;2. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China) |
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Abstract: | Single-crystalline BaCO3 nanowires were successfully synthesized in a reverse micelle modified solvothermal method. The reverse micelle in Oleie acid/n-octane/water system was proved to work as template to guide the growth of BaCO3 along 1-dimension. The samples were characterized with X- ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). Results show that the BaCO3 nanowires are single-crystalline and have a uniform structure with diameters between 80 and 200 nm and lengths between hundreds of nanometers and several microns. And the formation mechanism of BaCO3 was discussed. |
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Keywords: | BaCO3 nanowires reverse micelle |
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