| 原料体系对Ti3SiC2合成过程中相组成和显微结构的影响 |
| |
| 引用本文： | 袁蝴蝶,尹洪峰,陈盼军,卢琳琳.原料体系对Ti3SiC2合成过程中相组成和显微结构的影响[J].兵器材料科学与工程,2012,35(1):50-54. |
| |
| 作者姓名： | 袁蝴蝶 尹洪峰 陈盼军 卢琳琳 |
| |
| 作者单位： | 西安建筑科技大学材料科学与工程学院,陕西西安7 10055;西安建筑科技大学材料科学与工程学院,陕西西安7 10055;西安建筑科技大学材料科学与工程学院,陕西西安7 10055;西安建筑科技大学材料科学与工程学院,陕西西安7 10055 |
| |
| 基金项目： | 陕西省重点学科建设专项资金 |
| |
| 摘 要： | 分别以粉末钛粉、硅粉、石墨和钛粉、碳化硅、石墨为原料,采用热压烧结法制备Ti3SiC2材料。借助XRD和SEM手段研究原料体系和烧结温度对试样相组成、致密化程度和显微结构的影响,并分析反应烧结机理。结果表明,随着温度的升高,钛粉-硅粉-石墨体系较钛粉-碳化硅-石墨体系合成出的块体材料纯度更高,且质量分数可以达到72.29%。
|
| 关 键 词： | Ti3SiC2 热压烧结 相组成 显微结构 反应机理 |
Influence of raw material system on phase constituent and microstructure during Ti3SiC2 preparation |
| |
| YUAN Hudie,YIN Hongfeng,CHEN Panjun,LU Linlin.Influence of raw material system on phase constituent and microstructure during Ti3SiC2 preparation[J].Ordnance Material Science and Engineering,2012,35(1):50-54. |
| |
| Authors: | YUAN Hudie YIN Hongfeng CHEN Panjun LU Linlin |
| |
| Affiliation: | (School of Materials Science & Engineering,Xi′an University of Architecture & Technology,Xi′an 710055,China) |
| |
| Abstract: | The Ti3SiC2 ceramic material was synthesized by hot-pressing sintering processing with Ti,Si,C and Ti,SiC,C powders as raw materials.The effects of raw material system and sintering temperature on the phase constituent,densification and microstructure of samples were studied by XRD and SEM,and the reaction mechanism was analyzed,as well.The results show that with temperature increasing,the purity of the Ti3SiC2 material prepared using Ti,Si,C system is higher than that using Ti,SiC,C system,and the purity can reach 72.29%. |
| |
| Keywords: | titanium silicon carbide hot pressing phase constituent microstructure reaction mechanism |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
