| 三七中人参皂苷Rh1的分离与纯化 |
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| 引用本文： | 李龙华,富瑶瑶,石岭,许郁峰,鱼红闪,金凤燮. 三七中人参皂苷Rh1的分离与纯化[J]. 大连工业大学学报, 2011, 30(1): 23-25 |
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| 作者姓名： | 李龙华 富瑶瑶 石岭 许郁峰 鱼红闪 金凤燮 |
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| 作者单位： | 李龙华,LI Long-hua(大连工业大学生物工程学院,辽宁大连,116034;大连生生绿谷生物工程有限公司,辽宁大连,116023);富瑶瑶,石岭,许郁峰,鱼红闪,金凤燮,FU Yao-yao,SHI Ling,XU Yu-feng,YU Hong-shan,JIN Fang-fan(大连工业大学生物工程学院,辽宁大连,116034) |
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| 基金项目： | 国家自然科学基金，辽宁省教育厅创新团队项目 |
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| 摘 要： | 为了得到纯净的、具有较高生理和药理活性的单体人参皂苷Rh1,从三七中提取总皂苷,并对三七总皂苷进行分离纯化获得人参皂苷Rh1单体.分别经过乙醇浸提、石油醚脱脂、水饱和正丁醇萃取、大孔吸附树脂脱糖脱色及硅胶层析,从三七总皂苷中分离得到人参皂苷Rh1.结果表明,1 000 g三七干燥根经醇提、脱脂、萃取和脱糖脱色可制得三七...
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| 关 键 词： | 三七 人参皂苷 硅胶层析 高效液相色谱 |
Separation and purification of ginsenoside Rh1 in Panax notoginseng |
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| LI Long-hua,FU Yao-yao,SHI Ling,XU Yu-feng,YU Hong-shan,JIN Fang-fan. Separation and purification of ginsenoside Rh1 in Panax notoginseng[J]. Journal of Dalian Dalian Polytechnic University, 2011, 30(1): 23-25 |
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| Authors: | LI Long-hua FU Yao-yao SHI Ling XU Yu-feng YU Hong-shan JIN Fang-fan |
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| Affiliation: | LI Long-hua1,2,FU Yao-yao1,SHI Ling1,XU Yu-feng1,YU Hong-shan1,JIN Fang-fan11.School of Bioengineering,Dalian Polytechnic University,Dalian 116034,China;2.Dalian Groeen Bio-Tech Company Limited,Dalian 116023,China |
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| Abstract: | The ginsenoside Rh1 in Panax notoginseng was isolated by silica gel chromatography.76.2 g total notoginsenoside was obtained from 1 kg Panax notoginseng,the yield of total notoginsenoside was about 7.62%.0.36 g ginsenoside Rh1 was separated from 25 g total notoginsenoside by silica gel chromatography using chloroform and methanol at 8.5∶1.5 as the mobile phase,the yield of ginsenoside Rh1 was 1.44%,the purity was 66.08% detecting by HPLC. |
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| Keywords: | Panax notoginseng ginsenoside Rh1 silica gel chromatography HPLC |
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