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Synthesis of ordered carbon replicas by using Y-zeolite as template in a batch reactor
Authors:Arnd Garsuch
Affiliation:Institut für Technische Chemie, Universität Leipzig, Linnéstr. 3, D-04103 Leipzig, Germany
Abstract:Ordered carbon material that preserves the structural regularity of the parent zeolite template was synthesized by using ethylene as carbon source and HY-zeolite in a batch reactor. The obtained carbons exhibit a high degree of microporosity having BET surface areas between 1400 and 2400 m2/g. The morphology and structure of the prepared carbon materials were investigated by elemental analysis, X-ray diffraction measurements, scanning electron microscopy and nitrogen adsorption. The results were compared with the parent zeolite template. The carbonization procedure of precursor-encapsulated samples was investigated by thermal analysis and it has been found that the resulting quality of the ordered carbons strongly depends on the heat treatment of the composite material.
Keywords:Porous carbon  Carbonization  Adsorption  Porosity
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