Synthesis of pure nanocrystalline ZrO2 via a simple sonochemical-assisted route |
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| Affiliation: | 1. Department of Materials Science and Nano Technology, Yogi Vemana University, Kadapa 516003, India;2. Department of Physics, Yogi Vemana University, Kadapa 516003, India;1. Egyptian Petroleum Research Institute (EPRI), 11727 Cairo, Egypt;2. Chemistry Department, Faculty of Science, El-Zagazig University, Egypt;1. Department of Mechanical Engineering, S.R.K.R. Engineering College, Bhimavaram 534204, Andhra Pradesh, India;2. Department of Mechanical Engineering, University College of Engineering (A), Andhra University, Visakhapatnam 530003, Andhra Pradesh, India;1. Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan, P.O. Box 87317-51167, Iran;2. Environmental Technology Division, School of Industrial Technology, Universiti Sains Malaysia, 11800, Minden, Penang, Malaysia |
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| Abstract: | Pure nanocrystalline zirconia was synthesized via a sonochemical-assisted method based on the reaction between zirconyl nitrate and propylenediamine. Here, propylenediamine for the first time was used as precipitating agent to fabricate nanocrystalline zirconia via a sonochemical-assisted method. The effect of solvent and concentration of propylenediamine on the morphology and crystallite size was investigated. It was shown that morphology and crystallite size of the as-synthesized products could be greatly affected by these parameters. The as-prepared products were characterized by SEM and TEM images, XRD patterns, FT-IR and EDS spectroscopy. |
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| Keywords: | Zirconia Sonochemical Nanostructures Propylenediamine |
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