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铋碳共掺杂二氧化钛介孔光催化剂的制备及其表征
引用本文:孟艳玲,王伟,曲雅妮. 铋碳共掺杂二氧化钛介孔光催化剂的制备及其表征[J]. 化学工程师, 2009, 23(7): 20-22,55
作者姓名:孟艳玲  王伟  曲雅妮
作者单位:上海实业振泰化工有限公司,上海,201400;同济大学,土木工程学院,上海,200092;华东师范大学,化学系,上海,201402
摘    要:以吡啶为碳源,Bi(NO3)3·5H2O为铋源,结合溶胶-凝胶和高温陈化法制备出BiC共掺杂型TiO2光催化剂。利用紫外-可见漫反射光谱(UV—Vis)、X射线衍射(XRD)、N2吸附-脱附等温曲线(BET)对不同条件下制备出的样品进行了表征。结果表明:铋碳共掺杂TiO2催化剂具有典型的介孔结构;在可见光下对污染物靛红溶液有显著的降解效果;不同的煅烧温度及掺杂配比对催化剂光催化性能也有不同程度的影响。

关 键 词:TiO2  铋碳共掺杂  溶胶凝胶法  共沉淀法

Preparation and characterization of (Bi,C)-codoped TiO_2 mesopore photocatalyst
MENG Yan-ling,WANG wei,QU Ya-ni. Preparation and characterization of (Bi,C)-codoped TiO_2 mesopore photocatalyst[J]. Chemical Engineer, 2009, 23(7): 20-22,55
Authors:MENG Yan-ling  WANG wei  QU Ya-ni
Affiliation:1.Shanghai Zhentai Chemical General Factory;Shanghai 201400;China;2.School of Civil Engineering;Tongji University;Shanghai 200092;3.Department of Chemistry;East China Normal University;Shanghai 201402;China
Abstract:Pyridine and bismuth nitrate were used as precursors of the dopant.(Bi,C)-TiO2 photocatalyst codoped with metal and non-metal elements was successfully prepared by employing sol-gel method and hightemperature aging.The different codoping powders were characterized by UV-vis absorption spectroscopy(UV-vis),X-ray diffraction(XRD) and N2 adsorption-desorption isotherms.The results indicated that(Bi,C)-doped TiO2 has typical mesopore structure and showd satisfying photocatalytic efficiency on the degradation of...
Keywords:TiO2  TiO2  (Bi,C)-codoped  sol-gel method  coprecipitation method
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