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Preparation and Characterization of Fe2O3/Al2O3 Nano-composites
Authors:LIU Mei  YU Wen-xue  LI Hai-bo  XU Shi-chong  ZHANG Xiao-fen
Affiliation:1. College of Physics,Jilin Normal University,Siping 136000,China
2. College of Materials Science and Engineering,Jilin University,Changchun 130023,China
3. College of Physics,Jilin Normal University,Siping 136000,China;State Key Laboratory of Superhard Materials,Jilin University,Changchun 130012,China
Abstract:Al2O3/Fe2O3 nano-composites were prepared by sol-gel route. The effect of Fe2O3 content on the structure, grain size and characterization of the composite were investigated through X-ray diffraction and M(o)ssbauer spectrum. The X-ray diffraction results show that Al2O3/Fe2O3 nano-composites with the Fe2O3, content of 40 wt% can be obtained after heat-treated at 900℃. The M(o)ssbauer effect results show that all samples exhibit clear super-paramagnetic phenomenon. Particles grow and defects reduce with the increasing of Fe2O3 conteni and some α-Fe2O3 stay magnetic order.
Keywords:nano-composites  XRD  Mssbauer effect
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